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Solvent casting was completed utilizing a casting knife applicator from Elcometer (Rochester Hills, Michigan, North The united states) on heat-resistant borosilicate glass. All of the ways were being completed in a chemical laboratory the place ambient disorders of 18° ± two °C and R.H. twenty ± five% had been pointed out. The residual dampness written content during the films just after drying was measured utilizing Karl Fischer titration.
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Determine ten exhibits a comparison of agent surface morphology before bonding and following the fracture. The debonded fracture surfaces show local internet sites of chain scissions or pull-outs resulting from fracture.
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Schematic illustration contrasting mechanisms of interface molecular interpenetration (a) Polymer self-adhesion produced by molecular diffusion at temperatures near or previously mentioned Tg.
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